The choice of filter medium for a particular operation demands considerable experience.
FILTER MEDIA
The
choice of filter medium for a particular operation demands considerable
experience. In clarification, high filtration rates and the retention of fine
particles are opposing requirements. Permeability and retentive capacity can be
deter-mined and used to guide small-scale experiments with the materials to be
fil-tered, facilities for which are often made available by filter
manufacturers. Other relevant factors are the contamination of the filtrate by
the medium and associated housing, the adsorption of materials from solutions,
and, where necessary, the ability of the medium to withstand repeated
sterilization.
In
cake filtration, the medium must oppose excessive penetration and promote the
formation of a junction with the cake of high permeability. The medium should
also give free discharge of cake after washing and dewatering.
Rigid Media
Rigid
media may be either loose or fixed. The former is exemplified by the deposition
of a filter aid on a suitable support. Filtration characteristics are gov-erned
mainly by particle size, size distribution, and shape in a manner described
earlier. These factors may be varied for different filtering requirements.
Fixed
media vary from perforated metals used for coarse straining to the removal of
very fine particles with a sintered aggregate of metal, ceramic, plastic, or
glass powder. The size, size distribution, and shape of the powder particles
together with the sintering conditions control the size and distribution of the
pores in the final product. The permeability may be expressed in terms of the
constant given in equation (1). Alternatively, the medium may be charac-terized
by air permeability. The maximum pore size, which is important in the selection
of filters for sterilization, may be determined by measuring the pres-sure
difference required to blow a bubble of air through the medium while it
supports a column of liquid with a known surface tension. Full details of
methods used for the measurement of air permeability and maximum pore diameter
are given in British Standard BS 1752:1963.
Flexible
media may be woven or unwoven. Filter media woven from cotton, wool, synthetic
and regenerated fibers, glass, and metal fibers are used as septa in cake
filtration. Cotton is most widely used, while nylon is predominant among synthetic
fibers. Terylene is a useful medium for acid filtration. Pene-tration and cake
discharge are influenced by twisting and plying of fibers and by the adoption
of various weaves such as duck and twill. The choice of a particular cloth
often depends on the chemical nature of the slurry.
Nonwoven
media occur in the form of felts and compressed cellulose pulps and are used
for clarification by depth filtration. A disadvantage, unless carefully
prepared, is the loss of fibrous material from the downstream side of the
filter. The application of sheet media has already been discussed. High wet
strength is conferred on paper sheets by resin impregnation. An alternative
manufacture employs asbestos fibers supported in a cellulose framework.
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